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- Publisher
- Wiley
- Copyright
- © 2019 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim
- eISSN
- 2366-7486
- DOI
- 10.1002/adsu.201800084
- Publisher site
- See Article on Publisher Site
Abstract
Silicon‐on‐insulator (SOI) microring resonators coated with tetrasulfide‐functionalized mesoporous silica (MPS) (S4‐MPS) are reported as sensors to detect Pb(II) ions in aqueous solutions from 10 ppb to 1 ppm. The sensors are based on the interaction of the evanescent field of the guided light with the functionalized mesoporous silica films. Upon absorption of metal ions, the resonant wavelengths of the microresonators shift due to the increased refractive index of the film. The sensors are exposed to aqueous solutions of Pb(II) ions at different concentrations and time‐resolved absorption–desorption curves are obtained. The concentrations of Pb(II) ions are determined using the Lorentz–Lorenz model. It is found that two distinct binding sites with different affinities for Pb(II) are present in the S4‐MPS silica films, corresponding to tetrasulfide groups and, likely, silanol groups. The number of available binding sites corresponds to 1/25 of the total number of S4‐groups. Equilibrium constants for absorption of Pb(II) to both binding sites are obtained from the rate constants for the absorption and desorption processes. The initial absorption rates depend linearly on the concentration of Pb(II) and are used to determine the 3σ limit of detection as 58 ppbm in deionized water and 350 ppbm in tap water.
Journal
Advanced Sustainable Systems – Wiley
Published: Jan 1, 2019
Keywords: ; ; ; ; ; ;