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ABILITY OF TEREPHTHALATE (TA) TO MEDIATE EXCHANGE COUPLING IN TA-BRIDGED COPPER(II), NICKEL(II), COBALT(II) AND MANGANESE(II) DINUCLEAR COMPLEXESJournal of The Chemical Society-dalton Transactions
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Metal–radical approach to high spin molecules: a pentanuclear µ-cyano CrIIINiII(radical)2 complex with a low-lying S = 9 ground stateChemical Communications
A novel complex [Cu(NnpPy)2(HlTCB)(H1O)]·2H2O (NITpPy = 2‐(pyrid‐4′‐yl)‐4,4,5,5‐tetramethyl‐1, 3‐dioxoimidazoline; H2TCB = 1, 5‐dicarboxybenzene carboxylic‐2, 4‐diacid) has been synthesized and characterized by X‐ray crystallography analysis. The crystal structure consists of infinite chains of Cu‐(NITpPy)2(H2O) units linked by H2TCB ligands. The complex crystallizes in triclinic system with space group PI. Crystal data: a = 1.0594(2) nm, b = 1.3830(3) nm, c = 1.5551(3) nm, a = 67.75(3)°, β = 89.83(3)°, γ = 70.54(3)°. The variable magnetic susceptibility studies lead to magnetic coupling constant values of J1= −11.18 cm‐1 (Cu—Rad) and J2 = −4.06 cm−1 (Cu—Cu).
Chinese Journal of Chemistry – Wiley
Published: May 1, 2003
Keywords: ; ; ; ;
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