Access the full text.
Sign up today, get DeepDyve free for 14 days.
Loading next page...
/lp/wiley/synthesis-and-crystal-structure-of-a-new-salt-of-the-water-stable-yTO9GXjh8G
References (13)
-
R. Mercier, J. Malugani, B. Fahys, J. Douglande, G. Robert (1982)
Synthese, structure cristalline et analyse vibrationnelle de l'hexathiohypodiphosphate de lithium Li4P2S6Journal of Solid State Chemistry, 43
-
H. Falius (1968)
Hexathiohypophosphate, Salze einer neuen Säure des PhosphorsZeitschrift für anorganische und allgemeine Chemie, 356
-
A. El-Meligi (2004)
Investigation of MnPS3 intercalates with pyridinium ionMaterials Chemistry and Physics, 84
-
T. Fincher, G. Lebret, D. Cleary (1998)
Single-Crystal Structure Determination of Na4P2S6·6H2OIEEE Journal of Solid-state Circuits, 141
-
I. Lagadic, P. Lacroix, R. Clement (1997)
Layered MPS3 (M = Mn, Cd) Thin Films as Host Matrixes for Nonlinear Optical Material ProcessingChemistry of Materials, 9
-
M. Burla, R. Caliandro, M. Camalli, B. Carrozzini, G. Cascarano, L. Caro, C. Giacovazzo, G. Polidori, R. Spagna (2005)
SIR2004: an improved tool for crystal structure determination and refinementJournal of Applied Crystallography, 38
-
Yuandong Wu, W. Bensch (2009)
Syntheses, Crystal Structures and Spectroscopic Properties of Ag2Nb[P2S6][S2] and KAg2[PS4].ChemInform, 40
-
M. Armand, J. Tarascon (2008)
Building better batteriesNature, 451
-
A. Banister, W. Clegg, Wendy Gill (1987)
X-Ray crystal structures of some lithium aryl thiolates: monomeric [o-MeC6H4SLi·(NC5H5)3], chain [PhSLi·(NC5H5)2]∞, and the unique folded ladder of [PhCH2SLi·NC5H5]∞ with Li–S rungsJournal of The Chemical Society, Chemical Communications
-
O. Mys, I. Martynyuk-Lototska, A. Grabar, R. Vlokh (2009)
Acoustic and elastic properties of Sn2P2S6 crystalsJournal of Physics: Condensed Matter, 21
-
G. Sheldrick (2008)
A short history of SHELX.Acta crystallographica. Section A, Foundations of crystallography, 64 Pt 1
-
M. Gjikaj, C. Ehrhardt (2007)
New Hexachalcogeno–Hypodiphosphates of the Alkali Metals: Synthesis, Crystal Structure and Vibrational Spectra of the Hexathiodiphosphate(IV) Hydrates K4[P2S6] · 4 H2O, Rb4[P2S6] · 6 H2O, and Cs4[P2S6] · 6 H2OZeitschrift für anorganische und allgemeine Chemie, 633
-
F. Allen, T. Singh, D. Watson, L. Brammer, A. Orpen, Robin Taylor (1987)
Tables of bond lengths determined by X-ray and neutron diffraction. Part 1. Bond lengths in organic compoundsJournal of The Chemical Society-perkin Transactions 1
- Publisher
- Wiley
- Copyright
- "Copyright © 2014 Wiley Periodicals, Inc."
- ISSN
- 1042-7163
- eISSN
- 1098-1071
- DOI
- 10.1002/hc.21140
- Publisher site
- See Article on Publisher Site
Abstract
A new rare example of a synthetic route in solution to the hexathiohypodiphosphate anion P2S64− is presented. Starting from P4S3, Li2S, and elemental sulfur in pyridine, this reaction yields yellow block‐shaped crystals of [py2Li]4[P2S6] · 2 py (1). The molecular structure of this hitherto unknown compound was determined by single crystal X‐ray diffraction and reveals a heteronorbornane skeleton within the Li4P2S6 entity.
Journal
Heteroatom Chemistry – Wiley
Published: Mar 1, 2014