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2,4‐Di‐t‐butyl‐6‐methylphenylphosphonous dichloride reacted with chloroform in the presence of lithium diisopropylamide to give (2,4‐di‐t‐butyl‐6‐methylphenyl) (dichloromethyl) (1,2,2‐trichloroethenyl)phosphine. The structure of this phosphine was analyzed by X‐ray crystallography. This phosphine further reacted with butyllithium to give (1‐butylpentylidene)(2,4‐di‐t‐butyl‐6‐methylphenyl)phosphine bearing a low‐coordinated phosphorus atom. © 1996 John Wiley & Sons, Inc.
Heteroatom Chemistry – Wiley
Published: Jan 1, 1996
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