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- Publisher
- Wiley
- Copyright
- © 2021 Wiley‐VCH GmbH
- ISSN
- 2193-5807
- eISSN
- 2193-5815
- DOI
- 10.1002/ajoc.202100492
- Publisher site
- See Article on Publisher Site
Abstract
A convenient and efficient synthetic protocol for the preparation of pyrimidoquinazolinone through Pd(II)‐catalyzed carbonylative cyclization of N‐aryl‐2‐aminopyrimidines with Mo(CO)6 as carbon monoxide source is established. A series of 6H‐pyrimido[2,1‐b]quinazolin‐6‐one derivatives were obtained in good yields. The scale‐up synthesis was investigated.
Journal
Asian Journal of Organic Chemistry – Wiley
Published: Nov 1, 2021
Keywords: Pd(II)-catalyzed; carbonylative; cyclization; molybdenum hexacarbonyl; pyrimidoquinazolinone