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Phosphaalkynes, RCP (R = But, Adamantyl), add across the RhRh double bond of [Rh2Cp 2*(CO)2] to give either [Rh2Cp 2*(μ‐CO)(COPCR)] or [Rh2Cp 2*(CO){PCRC(O)CRP}] depending on the stoichiometry of the reaction (Cp* = η5‐C5Me5). The structures of these complexes have been elucidated by NMR spectroscopy and by a single crystal X‐ray study on [Rh2Cp 2*(CO){PCAdC(O)CPAd}]. Small amounts of the 1,3‐diphosphacyclobutadiene complexes [RhCp*(P2C2R2)] and the trinuclear compound [Rh3Cp 3*(CO)2] are also formed in these reactions. The reactions of RCP with [CoRhCp2*(CO)2] are also described. A preliminary account of part of this work has appeared in J. Chem. Soc., Chem. Commun., 1987, 658.
Heteroatom Chemistry – Wiley
Published: Jan 1, 1991
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