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CHINESE JOURNAL OF CHEMISTRY Vol. 31 No. 7 July 2013 Pages 865—972 COVER PICTURE The cover picture shows an efficient and cost-effective method for the preparation of fluorinated conjugated enynes. The method was compatible with a variety of functional groups such as chloride, amine, cyano and ester group. The method could also be extended to the coupling of (R,Z)-3- (2-chloro-1,2-difluorovinyl)-4-alkyloxazolidin-2-one (3) with moderate yields. More details are discussed in the article by Shen et al. on page 901—907. COMMUNICATION Nickel-Catalyzed ortho-Selective Hy- NiCl 6H O (5 mol%) drodefluorination of N-Containing Het- 2 2 Zn (10 mol%) N F erocycle-Polyfluoroarenes n F Et SiH Phen (5 mol%) DMF, 100 C n = 1 - 4 n = 1 - 4 10 examples An effective and facile method for preparation of partially fluorinated aromatics via Nickel catalyzed, chelation-assisted ortho selective hydrodefluorination of polyfluoro- Yi He, Zhao Chen, Chun-Yang He, arnes with triethylsilane has been developed, in which N-containing heterocycles were Xingang Zhang* used as directing groups. 868 © 2013 SIOC, CAS, Shanghai, & WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim Chin. J. Chem. 2013, 31, 868—871 FULL PAPERS OBz Highly Stereoselective and One-Pot LiHMDS SO Ph (PhSO ) CHF RCHO++ BzCl
Chinese Journal of Chemistry – Wiley
Published: Jul 1, 2013
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