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- Publisher
- Wiley
- Copyright
- Copyright © 2016 Wiley Subscription Services, Inc., A Wiley Company
- ISSN
- 0108-7673
- eISSN
- 1600-5724
- DOI
- 10.1107/S2053273315024055
- pmid
- 26919377
- Publisher site
- See Article on Publisher Site
Abstract
Two methods for scaling of multicrystal data collected in time‐resolved photocrystallography experiments are discussed. The WLS method is based on a weighted least‐squares refinement of laser‐ON/laser‐OFF intensity ratios. The other, previously applied, is based on the average absolute system response to light exposure. A more advanced application of these methods for scaling within a data set, necessary because of frequent anisotropy of light absorption in crystalline samples, is proposed. The methods are applied to recently collected synchrotron data on the tetra‐nuclear compound Ag2Cu2L4 with L = 2‐diphenylphosphino‐3‐methylindole. A statistical analysis of the weighted least‐squares refinement residual terms is performed to test the importance of the scaling procedure.
Journal
Acta Crystallographica Section A Foundations of Crystallography – Wiley
Published: Mar 1, 2016
Keywords: ; ; ; ;