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An efficient and green method to the synthesis of N‐protected o‐hydroxylphenyl α‐amino‐alkylphosphonic monoesters is described. It consists of the three‐component Mannich‐type reaction of phosphoramides, carbonyl compounds (aldehydes or ketones), and 2‐chlorobenzo(1,3,2) diox‐aphospholes under solvent‐free and catalyst‐free conditions, followed by hydrolysis. © 2008 Wiley Periodicals, Inc. Heteroatom Chem 19:596–601, 2008; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/hc.20483
Heteroatom Chemistry – Wiley
Published: Sep 1, 2008
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