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Starting from an organic multiyne, three steps are normally needed for the preparation of non‐β‐phosphonium functionalized rhoda‐ and irida‐carbolong complexes. Herein, a one‐pot strategy, by mixing a multiyne, a nucleophile, and RhCl(CO)(PPh3)2/AgBF4 or [Ir(CH3CN)(CO)(PPh3)2]BF4, was developed to achieve a series of β‐functionalized rhoda‐ and irida‐carbolong complexes. The β‐substituents in these complexes can be various C‐, N‐ and O‐centered groups, dependent on the nucleophiles used. This strategy provides a new convenient route to construct carbolong complexes, which is important for the further development of carbolong chemistry.
Chinese Journal of Chemistry – Wiley
Published: Aug 1, 2022
Keywords: Carbolong chemistry; Metallacycles; Rhodium; Iridium; Tridentate ligands
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