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Reaction of 1‐chloro‐2,2‐dimethoxyethane with sodium azide affords 1‐azido‐2,2‐dimethoxyethane which, upon treatment with triphenylphosphine followed by aromatic aldehydes, alkyl bromides, or isocyanates, gives the corresponding dimethyl α‐arylimino‐, α‐alkylamino‐, and α‐carbodiimido‐acetals, respectively, in good to excellent yields.
Heteroatom Chemistry – Wiley
Published: Jan 1, 1994
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