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2‐Benzothiazolyl‐ N ‐(arenesulfonyl)‐sulfinimidoyl fluorides

2‐Benzothiazolyl‐ N ‐(arenesulfonyl)‐sulfinimidoyl fluorides 2‐Benzothiazolyl‐N‐(arenesulfonyl)‐sulfinimidoyl fluorides were synthesized by the treatment of benzothiazolyl‐2‐sulfur trifluoride with sulfonamides. The reaction of 2‐benzothiazolyl‐N‐ (p‐toluenesulfonyl)‐sulfinimidoyl fluoride with tert‐ butylamine and morpholine gave 2‐benzothiazolyl‐ N‐(arenesulfonyl)‐sulfinimidoyl amides. The reaction of 2‐benzothiazolyl‐N‐(p‐toluenesulfonyl)‐sulfinimi‐ doyl fluoride or 2‐benzothiazolyl‐15N‐(p‐tosyl)sul‐ finimidoyl fluoride with S‐trimethylsilylbenzenethiol gave di(benzothiazolyl‐2) disulfide, fluorotrimethylsi‐ lane and N,N′‐bis(p‐toluenesulfonyl)‐N,N′‐bis(phenyl‐ thio)‐hydrazine or 15N,15N′‐bis(p‐toluenesulfonyl)‐15N, 15N′‐bis(phenylthio)‐hydrazine, respectively. © 2005 Wiley Periodicals, Inc. Heteroatom Chem 16:352–356, 2005; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/hc.20102 http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Heteroatom Chemistry Wiley

2‐Benzothiazolyl‐ N ‐(arenesulfonyl)‐sulfinimidoyl fluorides

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References (18)

Publisher
Wiley
Copyright
Copyright © 2005 Wiley Periodicals, Inc.
ISSN
1042-7163
eISSN
1098-1071
DOI
10.1002/hc.20102
Publisher site
See Article on Publisher Site

Abstract

2‐Benzothiazolyl‐N‐(arenesulfonyl)‐sulfinimidoyl fluorides were synthesized by the treatment of benzothiazolyl‐2‐sulfur trifluoride with sulfonamides. The reaction of 2‐benzothiazolyl‐N‐ (p‐toluenesulfonyl)‐sulfinimidoyl fluoride with tert‐ butylamine and morpholine gave 2‐benzothiazolyl‐ N‐(arenesulfonyl)‐sulfinimidoyl amides. The reaction of 2‐benzothiazolyl‐N‐(p‐toluenesulfonyl)‐sulfinimi‐ doyl fluoride or 2‐benzothiazolyl‐15N‐(p‐tosyl)sul‐ finimidoyl fluoride with S‐trimethylsilylbenzenethiol gave di(benzothiazolyl‐2) disulfide, fluorotrimethylsi‐ lane and N,N′‐bis(p‐toluenesulfonyl)‐N,N′‐bis(phenyl‐ thio)‐hydrazine or 15N,15N′‐bis(p‐toluenesulfonyl)‐15N, 15N′‐bis(phenylthio)‐hydrazine, respectively. © 2005 Wiley Periodicals, Inc. Heteroatom Chem 16:352–356, 2005; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/hc.20102

Journal

Heteroatom ChemistryWiley

Published: Jan 1, 2005

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