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ISSN 0020-1685, Inorganic Materials, 2019, Vol. 55, No. 3, pp. 256–262. © Pleiades Publishing, Ltd., 2019. Russian Text © V.P. Isupov, I.A. Borodulina, R.N. Niyazova, N.V. Eremina, 2019, published in Neorganicheskie Materialy, 2019, Vol. 55, No. 3, pp. 283–289. Synthesis of Fine-Particle α-LiAlO via Heat Treatment of a Mechanically Activated Mixture of Gibbsite and Lithium Carbonate a, a a, b a V. P. Isupov *, I. A. Borodulina , R. N. Niyazova , and N. V. Eremina Institute of Solid State Chemistry and Mechanochemistry, Siberian Branch, Russian Academy of Sciences, ul. Kutateladze 18, Novosibirsk, 630128 Russia Novosibirsk State Technical University, pr. Marksa 20, Novosibirsk, 630073 Russia *e-mail: isupov@solid.nsc.ru Received May 12, 2018; revised October 4, 2018; accepted October 15, 2018 Abstract—We have found conditions for the synthesis of fine-particle phase-pure α-LiAlO via heat treat- ment of a mechanically activated mixture of gibbsite and lithium carbonate in air. The results demonstrate that, to synthesize α-LiAlO , the mechanical activation of the reaction mixture should cause no gibbsite amorphization and heat treatment in air should be performed in the range 650–700°C. Keywords: aluminum hydroxide, lithium carbonate, mechanical activation, thermal interaction DOI: 10.1134/S0020168519030099 INTRODUCTION Later, gamma-aluminum oxide was used as an alumi-
Inorganic Materials – Springer Journals
Published: Jun 5, 2019
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