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Carborane–Siloxanes: Synthesis and Properties. New Possibilities for Structure Control, 1
Monosubstituted B-chloro(organo)silylmethyl-o-carboranes have been synthesized for the first time by the reaction of o-carborane with chloromethyl(organo)chlorosilanes in the presence of catalytic amount of aluminum chloride. The reaction proceeds at temperature of 200–250°C under a pressure of 22–25 atm. A decrease in the number of chlorine atoms in the molecule of chloromethyl(organo)chlorosilane decreases the yield of the target product.
Doklady Chemistry – Springer Journals
Published: May 16, 2020
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