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- Publisher
- Springer Journals
- Copyright
- 2009 Pleiades Publishing, Ltd.
- ISSN
- 1063-7745
- eISSN
- 1562-689X
- DOI
- 10.1134/s1063774509020102
- Publisher site
- See Article on Publisher Site
Abstract
Abstract The pyridoxine complexes with zinc and cadmium sulfates are synthesized. The IR absorption spectra and thermal behavior of the synthesized compounds are described. Crystals of the [M(C8H11O3N)2(H2O)2]SO4 · 3H2O (M = Zn, Cd) compounds are investigated using X-ray diffraction. In the structures of both compounds, the M atoms are coordinated by the oxygen atoms of the deprotonated OH group and the CH2OH group retaining its own hydrogen atom, as well as by two H2O molecules, and have an octahedral coordination. The nitrogen atom of the heterocycle is protonated, so that the heterocycle acquires a pyridinium character. The cationic complexes form layers separated by the anions and crystallization water molecules located in between. The structural units of the crystals are joined together by a complex system of hydrogen bonds.
Journal
Crystallography Reports – Springer Journals
Published: Mar 1, 2009
Keywords: Crystallography and Scattering Methods