Access the full text.
Sign up today, get DeepDyve free for 14 days.
G.M. Sheldrick (1989)
SHELXTL PLUS, PC version
Doklady Chemistry, Vol. 380, Nos. 4–6, 2001, pp. 284–286. Translated from Doklady Akademii Nauk, Vol. 380, No. 5, 2001, pp. 639–641. Original Russian Text Copyright © 2001 by Palyulin, Emets, Potekhin, Lysov, Sumskaya, Zefirov. CHEMISTRY Synthesis and Crystal and Molecular Structure of 3,7-Dithenoyl-1,5-dimethyl-3,7-diazabicyclo[3.3.1]nonane V. A. Palyulin, S. V. Emets, K. A. Potekhin, A. E. Lysov, Yu. G. Sumskaya, and Academician N. S. Zefirov Received June 19, 2001 Previously, we described the synthesis and X-ray were refluxed in chloroform (30 mL) for 5 h. After diffraction analysis of a series of 3,7-diacyl-3,7-diaza- cooling, the mixture was treated with stirring with a sat- bicyclo[3.3.1]nonanes (1) existing in the chair–chair urated solution of KHCO , the organic layer was sepa- conformation [1–3]. In solutions, the antiparallel (ap) rated, the aqueous layer was extracted with chloroform orientation of substituents in these compounds tends to (2 · 10), the combined organic extracts were dried by change to the parallel (pa) orientation upon an increase Na SO , and the solvent was evaporated. The product 2 4 in the medium polarity or in the presence of salts of lan- thanum(III) coordinated to carbonyl groups. C(9) C(10) Me Me C(11) Me Me increase in e C(1)
Doklady Chemistry – Springer Journals
Published: Oct 12, 2004
Read and print from thousands of top scholarly journals.
Already have an account? Log in
Bookmark this article. You can see your Bookmarks on your DeepDyve Library.
To save an article, log in first, or sign up for a DeepDyve account if you don’t already have one.
Copy and paste the desired citation format or use the link below to download a file formatted for EndNote
Access the full text.
Sign up today, get DeepDyve free for 14 days.
All DeepDyve websites use cookies to improve your online experience. They were placed on your computer when you launched this website. You can change your cookie settings through your browser.