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Synthesis and Crystal and Molecular Structure of 3,7-Dithenoyl-1,5-dimethyl-3,7-diazabicyclo[3.3.1]nonane

Synthesis and Crystal and Molecular Structure of... Doklady Chemistry, Vol. 380, Nos. 4–6, 2001, pp. 284–286. Translated from Doklady Akademii Nauk, Vol. 380, No. 5, 2001, pp. 639–641. Original Russian Text Copyright © 2001 by Palyulin, Emets, Potekhin, Lysov, Sumskaya, Zefirov. CHEMISTRY Synthesis and Crystal and Molecular Structure of 3,7-Dithenoyl-1,5-dimethyl-3,7-diazabicyclo[3.3.1]nonane V. A. Palyulin, S. V. Emets, K. A. Potekhin, A. E. Lysov, Yu. G. Sumskaya, and Academician N. S. Zefirov Received June 19, 2001 Previously, we described the synthesis and X-ray were refluxed in chloroform (30 mL) for 5 h. After diffraction analysis of a series of 3,7-diacyl-3,7-diaza- cooling, the mixture was treated with stirring with a sat- bicyclo[3.3.1]nonanes (1) existing in the chair–chair urated solution of KHCO , the organic layer was sepa- conformation [1–3]. In solutions, the antiparallel (ap) rated, the aqueous layer was extracted with chloroform orientation of substituents in these compounds tends to (2 · 10), the combined organic extracts were dried by change to the parallel (pa) orientation upon an increase Na SO , and the solvent was evaporated. The product 2 4 in the medium polarity or in the presence of salts of lan- thanum(III) coordinated to carbonyl groups. C(9) C(10) Me Me C(11) Me Me increase in e C(1) http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Doklady Chemistry Springer Journals

Synthesis and Crystal and Molecular Structure of 3,7-Dithenoyl-1,5-dimethyl-3,7-diazabicyclo[3.3.1]nonane

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References (1)

Publisher
Springer Journals
Copyright
Copyright © 2001 by MAIK “Nauka/Interperiodica”
Subject
Chemistry; Chemistry/Food Science, general; Industrial Chemistry/Chemical Engineering
ISSN
0012-5008
eISSN
1608-3113
DOI
10.1023/A:1012328123335
Publisher site
See Article on Publisher Site

Abstract

Doklady Chemistry, Vol. 380, Nos. 4–6, 2001, pp. 284–286. Translated from Doklady Akademii Nauk, Vol. 380, No. 5, 2001, pp. 639–641. Original Russian Text Copyright © 2001 by Palyulin, Emets, Potekhin, Lysov, Sumskaya, Zefirov. CHEMISTRY Synthesis and Crystal and Molecular Structure of 3,7-Dithenoyl-1,5-dimethyl-3,7-diazabicyclo[3.3.1]nonane V. A. Palyulin, S. V. Emets, K. A. Potekhin, A. E. Lysov, Yu. G. Sumskaya, and Academician N. S. Zefirov Received June 19, 2001 Previously, we described the synthesis and X-ray were refluxed in chloroform (30 mL) for 5 h. After diffraction analysis of a series of 3,7-diacyl-3,7-diaza- cooling, the mixture was treated with stirring with a sat- bicyclo[3.3.1]nonanes (1) existing in the chair–chair urated solution of KHCO , the organic layer was sepa- conformation [1–3]. In solutions, the antiparallel (ap) rated, the aqueous layer was extracted with chloroform orientation of substituents in these compounds tends to (2 · 10), the combined organic extracts were dried by change to the parallel (pa) orientation upon an increase Na SO , and the solvent was evaporated. The product 2 4 in the medium polarity or in the presence of salts of lan- thanum(III) coordinated to carbonyl groups. C(9) C(10) Me Me C(11) Me Me increase in e C(1)

Journal

Doklady ChemistrySpringer Journals

Published: Oct 12, 2004

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