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Structure refinement of cadmium cerium(IV) phosphate Cd 0.5 Ce 2 (PO 4 ) 3

Structure refinement of cadmium cerium(IV) phosphate Cd 0.5 Ce 2 (PO 4 ) 3 Abstract Cadmium cerium orthophosphate Cd0.5Ce2(PO4)3 is synthesized by precipitation from aqueous solutions. The structure refinement from powder X-ray diffraction data is preceded by the sample preparation and structure solution. The refinement is carried out by the Rietveld method (ADP-2 diffractometer, Cu Kα radiation, Ni filter, 15° < 2θ < 120°, 2θ-scan step 0.02°, counting time 10 s per step). All calculations are carried out using the WYRIET program (version 3.3) within the sp. gr. P21/n. The structure is refined with anisotropic displacement parameters for cations and isotropic displacement parameters for oxygen atoms. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Crystallography Reports Springer Journals

Structure refinement of cadmium cerium(IV) phosphate Cd 0.5 Ce 2 (PO 4 ) 3

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References (7)

Publisher
Springer Journals
Copyright
2005 Pleiades Publishing, Inc.
ISSN
1063-7745
eISSN
1562-689X
DOI
10.1134/1.2132396
Publisher site
See Article on Publisher Site

Abstract

Abstract Cadmium cerium orthophosphate Cd0.5Ce2(PO4)3 is synthesized by precipitation from aqueous solutions. The structure refinement from powder X-ray diffraction data is preceded by the sample preparation and structure solution. The refinement is carried out by the Rietveld method (ADP-2 diffractometer, Cu Kα radiation, Ni filter, 15° < 2θ < 120°, 2θ-scan step 0.02°, counting time 10 s per step). All calculations are carried out using the WYRIET program (version 3.3) within the sp. gr. P21/n. The structure is refined with anisotropic displacement parameters for cations and isotropic displacement parameters for oxygen atoms.

Journal

Crystallography Reports – Springer Journals

Published: Nov 1, 2005

Keywords: Crystallography and Scattering Methods

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