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Abstract X-ray diffraction studies of sillenite Bi24V2O40 single crystals grown by the hydrothermal method are performed for a separate crystal and powdered crystals. It is found that the composition of the two specimens is described by the (Bi24 − x ▭ x )[Bi 3+ y V 5+1−y ]2 O40 general formula with completely populated oxygen sites but differs in the content of vacancies at the bismuth site (this was established for the first time) and the Bi: V ratio at the tetrahedral site. The structural models of all the vanadium-containing sillenites reported in the literature are considered, and the possibility that Bi atoms are located at the centers of BiO4 tetrahedra is established.
Crystallography Reports – Springer Journals
Published: Mar 1, 2011
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