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- Publisher
- Springer Journals
- Copyright
- 2008 Pleiades Publishing, Ltd.
- ISSN
- 1063-7745
- eISSN
- 1562-689X
- DOI
- 10.1134/s1063774508060084
- Publisher site
- See Article on Publisher Site
Abstract
Abstract The structures of the ɛ-FeOOH, ɛ-FeOOD, and β-GaOOH phases, which belong to the InOOH structure type (the distorted TiO2 structure type), are determined using single-crystal X-ray diffraction analysis. The measurements are performed on Xcalibur CCD and CAD-4F diffractometers. The calculations are carried out in space group P21nm with the JANA2000 program. The crystals are twinned and form aggregates related by the rotation around the b axis through an angle close to 62°. In the same crystals, the merohedral twinning is characterized by the rotation around the c axis through an angle of 180°. The alternation of these twin domains in the bulk of the crystal determines the corresponding disordering of the hydrogen positions.
Journal
Crystallography Reports – Springer Journals
Published: Nov 1, 2008
Keywords: Crystallography and Scattering Methods