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Doklady Chemistry, Vol. 397, Part 1, 2004, pp. 149–152. Translated from Doklady Akademii Nauk, Vol. 397, No. 2, 2004, pp. 205–209. Original Russian Text Copyright © 2004 by Belyavskii, Lisichkin. CHEMISTRY Regularities of Chemical Modification of Tin(IV) and Copper(II) Oxide Surfaces by Arylsilanes S. G. Belyavskii and G. V. Lisichkin Presented by Academician Yu.A. Zolotov March 4, 2004 Received March 9, 2004 The influence of the key factors (the nature and the strates were determined by nitrogen adsorption under a functionality of the modifier, the presence of water) on constant pressure (145 and 70 m /g, respectively). the chemical modification of the surfaces of tin(IV) and The oxide surface was modified using commercially copper(II) oxides by arylsilanes with different types of available phenyltrichloro-, diphenyldichloro-, triphe- substitution were studied by Fourier Transform IR nylchloro-, phenyltriethoxy, and diphenyldiethoxysi- spectroscopy and thermal and elemental analyses. The lanes. The preparation of triphenylethoxysilane and hydrolytic and thermal stabilities of the grafted layers chemical modification of the oxide surface were carried were determined. out by a reported procedure [7]. IR spectra of the modified surfaces were measured The chemistry of surface modification has been best on a Perkin Elmer instrument in the reflection mode. developed
Doklady Chemistry – Springer Journals
Published: Oct 9, 2004
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