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- Publisher
- Springer Journals
- Copyright
- Copyright © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022
- ISSN
- 1380-2224
- eISSN
- 1573-4854
- DOI
- 10.1007/s10934-022-01250-0
- Publisher site
- See Article on Publisher Site
Abstract
Active metal agglomeration in heterogeneous catalysis is a crucial reason of catalyst deactivation. Consequently, many methods to inhibit the sintering by redispersing metal course have been widely studied. However, the redispersion conditions of catalysts with different structures may also be different. In our work, we prepared Pt/ZSM-5 and Pt@ZSM-5 catalysts to study that the redispersion of Pt under different pretreatment conditions. Characterizations demonstrate that only Pt@ZSM-5 (4R, 5O) implements Pt redispersion. The redispersion of Pt nanoparticles is due to the encapsulation constraint of the ZSM-5 as well as Ptδ+ species migrate in oxygen atmosphere at 500 °C, which are anchored to the –(–O–Si≡)y site in ZSM-5 by strong metal support interaction. Benefiting from highly dispersed active sites, Pt@ZSM-5 (4R, 5O) catalyst also shows excellently catalytic activity, stability and anti-carbon deposition ability for partial oxidation of methane (POM). The results provide ideas for the preparation of catalysts for high temperature oxidation reaction.
Journal
Journal of Porous Materials – Springer Journals
Published: Oct 1, 2022
Keywords: Agglomeration; Redispersion; Encapsulation; Strong metal support interaction; Partial oxidation of methane