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- Publisher
- Springer Journals
- Copyright
- 2017 The Polymer Society of Korea and Springer Sciene+Business Media Dordrecht
- ISSN
- 1598-5032
- eISSN
- 2092-7673
- DOI
- 10.1007/s13233-017-5026-8
- Publisher site
- See Article on Publisher Site
Abstract
Abstract Vinylphosphonic acid is homopolymerized with dimethylvinylphosphonate by radical polymerization using using UV light and photoinitiator Darocur 4265 (3 wt%). The molar ratio between vinylphosphonic acid and dimethylvinylphosphonate is varied between 1:1 and 4:1, respectively. The obtained homopolymer of vinylphosphonic acid and copolymers are characterized by Fourier transform infrared spectroscopy (FTIR), thermal analysis and size exclusion chromatography - multi angle laser light scattering. The polymerization by UV light is efficient and an average molar mass of 34,200 g/mol is obtained for poly(vinylphosphonic acid) and in the range from 12,700 to 19,120 g/mol for copolymers, which also have a good thermal stability until 320 °C. The polymers structure allows the formation of random coil conformation. The copolymers are tested as inhibitors against corrosion of iron in NaCl aqueous solution, and, as a result, it was shown that these copolymers exhibit promising anticorrosion properties.
Journal
"Macromolecular Research" – Springer Journals
Published: Mar 1, 2017