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- Publisher
- Springer Journals
- Copyright
- 2014 The Polymer Society of Korea and Springer Sciene+Business Media Dordrecht
- ISSN
- 1598-5032
- eISSN
- 2092-7673
- DOI
- 10.1007/s13233-014-2043-8
- Publisher site
- See Article on Publisher Site
Abstract
Abstract Graphene-reinforced poly(p-phenylene benzobisoxazole) (PBO) composite fibers were manufactured via dry-jet wet-spinning of PBO/graphene mixtures in poly(phosphoric acid) (PPA), which were reaction products prepared by the in situ polymerization of 4,6-diaminoresorcinol dihydrochloride and terephthaloyl chloride in the presence of PPA solvent and exfoliated graphene sheets. The content of graphene sheets in the as-spun fibers was adjusted to 0.0∼2.0 wt%. The molecular structure, crystalline order, and morphology of the as-spun fibers of pristine PBO and PBO/graphene composites were identified using FTIR, X-ray diffraction, and electron/optical microscopy. The thermal stability and tensile mechanical properties of the composite fiber with 0.2 wt% graphene were found to be significantly improved compared to the pristine PBO fiber.
Journal
"Macromolecular Research" – Springer Journals
Published: Mar 1, 2014