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γ-MnO2 for Li batteries: Part I. γ-MnO2: Relationships between synthesis conditions, material characteristics and performances in lithium batteriesJournal of Power Sources, 81
- Publisher
- Springer Journals
- Copyright
- Copyright © 2004 by IfI - Institute for Ionics
- Subject
- Chemistry; Biomedicine general; Analytical Chemistry; Physical Chemistry; Electrochemistry; Optical and Electronic Materials
- ISSN
- 0947-7047
- eISSN
- 1862-0760
- DOI
- 10.1007/BF02382818
- Publisher site
- See Article on Publisher Site
Abstract
The spinel LiMn2O4 is a very promising cathode material with economical and environmental advantages. LiMn2O4 materials have been synthesized by solid state method using γ-MnO2 as manganese source, and Li2CO3 or LiNO3 as Li sources. γ-MnO2 is a commercial battery grade electrolytic manganese dioxide (TOSOH-Hellas GH-S) and LiMn2O4 samples were synthesized at a calcinations temperature up to 800 °C. γ-MnO2 and LiMn2O4 samples were characterized by X-ray diffraction, thermal and electrochemical measurements. X-ray powder diffraction of as prepared LiMn2O4 showed a well-defined highly pure spinel single phase. The electrochemical performance of LiMn2O4 and its starting material γ-MnO2 was evaluated through cyclic voltammetry, galvanostatic (constant current charge-discharge cycling) The electrochemical properties in terms of cycle performance were also discussed.
Journal
Ionics – Springer Journals
Published: Mar 25, 2006