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ISSN 00125008, Doklady Chemistry, 2013, Vol. 448, Part 1, pp. 31–34. © Pleiades Publishing, Ltd., 2013. Original Russian Text © V.B. Sokolov, A.Yu. Aksinenko, T.V. Goreva, T.A. Epishina, I.V. Martynov, 2013, published in Doklady Akademii Nauk, 2013, Vol. 448, No. 3, pp. 310–313. CHEMISTRY Methyl Trifluoropyruvate in Cyclocondensation with 1,3Bis(nucleophiles) V. B. Sokolov, A. Yu. Aksinenko, T. V. Goreva, T. A. Epishina, and Corresponding Member of the RAS I. V. Martynov Received July 17, 2012 DOI: 10.1134/S0012500813010096 The directed synthesis of fivemembered heterocy MTFP 1 as available fluorinecontaining 1,2bis(elec clic systems by the cyclocondensation of 1,2bis(elec trophile) in cyclocondensation reactions with 1,3 trophiles) with 1,3bis(nucleophiles) is a topical task bis(nucleophiles) resulting in various heterocyclic of organic chemistry in spite of the well developed but derivatives of trifluoro2hydroxypropionic acid. continuously updated by new data methodology of The reaction of compound 1 with 1,3bis(nucleo these transformations. In our opinion, the present philes) was accomplished as a twostage cycloconden study is a new original evolution of this synthetic prac sation reaction: addition of bis(nucleophile) at highly tice as applied to the synthesis of trifluoromethylcon electrophilic C=O bond followed by heterocyclization taining fivemembered heterocyclic compounds. with methanol elimination. 6Amino1benzyluracil Methyl trifluoropyruvate (MTFP) derivatives,
Doklady Chemistry – Springer Journals
Published: Feb 16, 2013
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