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Deuterium or tritium labeling of brassinolide

Deuterium or tritium labeling of brassinolide ISSN 00125008, Doklady Chemistry, 2013, Vol. 448, Part 2, pp. 66–67. © Pleiades Publishing, Ltd., 2013. Original Russian Text © V.P. Shevchenko, I.Yu. Nagaev, N.F. Myasoedov, 2013, published in Doklady Akademii Nauk, 2013, Vol. 448, No. 6, pp. 668–669. CHEMISTRY V. P. Shevchenko, I. Yu. Nagaev, and Academician N. F. Myasoedov Received October 22, 2012 DOI: 10.1134/S0012500813020109 Labeling of biologically active compounds that do 15 min and the reaction temperature, from 180 to not contain moieties into which hydrogen isotopes are 260°С. The reaction was carried out in deuterium or efficiently introduced (for example, moieties with aro tritium gas at a pressure of 400 hPa. matic rings) is a problem. If the contact of molecules The best results were obtained with the use of 5% of such compounds with the support makes it possible Rh/Al O and 5% Pd/C, which led to the introduction 2 3 for activated hydrogen particles to efficiently interact of, on average, 0.6 and 0.3 deuterium atoms per brass with the substrate, labeled preparations with high inolide molecule, respectively. molar radioactivity can be obtained [1]. If the charges For the 5% Rh/Al O –Al O –brassinolide mixture, 2 3 2 3 that appear on polar http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Doklady Chemistry Springer Journals

Deuterium or tritium labeling of brassinolide

Shevchenko, V.; Nagaev, I.; Myasoedov, N.
Doklady Chemistry , Volume 448 (2) – Mar 12, 2013
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References (3)

Publisher
Springer Journals
Copyright
Copyright © 2013 by Pleiades Publishing, Ltd.
Subject
Chemistry; Chemistry/Food Science, general; Industrial Chemistry/Chemical Engineering
ISSN
0012-5008
eISSN
1608-3113
DOI
10.1134/S0012500813020109
Publisher site
See Article on Publisher Site

Abstract

ISSN 00125008, Doklady Chemistry, 2013, Vol. 448, Part 2, pp. 66–67. © Pleiades Publishing, Ltd., 2013. Original Russian Text © V.P. Shevchenko, I.Yu. Nagaev, N.F. Myasoedov, 2013, published in Doklady Akademii Nauk, 2013, Vol. 448, No. 6, pp. 668–669. CHEMISTRY V. P. Shevchenko, I. Yu. Nagaev, and Academician N. F. Myasoedov Received October 22, 2012 DOI: 10.1134/S0012500813020109 Labeling of biologically active compounds that do 15 min and the reaction temperature, from 180 to not contain moieties into which hydrogen isotopes are 260°С. The reaction was carried out in deuterium or efficiently introduced (for example, moieties with aro tritium gas at a pressure of 400 hPa. matic rings) is a problem. If the contact of molecules The best results were obtained with the use of 5% of such compounds with the support makes it possible Rh/Al O and 5% Pd/C, which led to the introduction 2 3 for activated hydrogen particles to efficiently interact of, on average, 0.6 and 0.3 deuterium atoms per brass with the substrate, labeled preparations with high inolide molecule, respectively. molar radioactivity can be obtained [1]. If the charges For the 5% Rh/Al O –Al O –brassinolide mixture, 2 3 2 3 that appear on polar

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Doklady Chemistry – Springer Journals

Published: Mar 12, 2013

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