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- Publisher
- Springer Journals
- Copyright
- Copyright © Pleiades Publishing, Ltd. 2020
- ISSN
- 0020-1685
- eISSN
- 1608-3172
- DOI
- 10.1134/S0020168520070080
- Publisher site
- See Article on Publisher Site
Abstract
This paper presents a detailed study of the magnetic and crystal structures of BaFe12 –xZnxO19 (0.25 ≤ x ≤ 1.5) Zn-substituted barium hexaferrite by Mössbauer spectroscopy, vibrating sample magnetometry, and X-ray diffraction. Partial heterovalent substitution of Zn2+ ions for Fe3+ ions demonstrates limited heterovalent isomorphism according to the scheme 2Fe3+ → Zn2+ + Fe4+, which satisfies the electroneutrality constraint. Mössbauer spectroscopy results indicate the presence of Fe4+ in the BaFe12 –xZnxO19 materials. The heterovalent isomorphous substitution limit has been determined to be x = 1.0. The formation of a zinc spinel has been shown to begin at x = 0.50 and its content increases with increasing zinc content. Data are presented on the predominant character of the substituent ion (Zn2+) distribution in the structure of barium hexaferrite. A correlation has been found between the chemical composition, phase separation, anisotropy of properties, and the temperature of the magnetic phase transition of BaFe12 –xZnxO19 (0.25 ≤ x ≤ 1.5).
Journal
Inorganic Materials – Springer Journals
Published: Jul 28, 2020