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Fundamental principles of polymeric materials
- Publisher
- Springer Journals
- Copyright
- 2009 The Polymer Society of Korea and Springer
- ISSN
- 1598-5032
- eISSN
- 2092-7673
- DOI
- 10.1007/BF03218648
- Publisher site
- See Article on Publisher Site
Abstract
Abstract Copolymers ofN-vinylpyrrolidone (NVP) comonomer with styrene (St), hydroxypropyl methacrylate (HPMA) and carboxyphenyl maleimide (CPMI) were synthesized by free radical polymerization using 2,2′-azobisisobutyronitrile (AIBN) initiator in 1,4-dioxane solvent. The copolymers formed were characterized by FTIR,1H NMR and13C NMR techniques and their thermal properties were studied by DSC and TGA. Copolymer composition was determined by1H NMR and/or by elemental analysis and monomer reactivity ratios (MRR) were estimated by the linear methods of Kelen-Tudos (K-T) and extended Kelen-Tudos (EK-T) and the non-linear approach. Copolymers of St and HPMA with NVP formed blocks of one of the monomer units, whereas alternating copolymers were obtained in CPMI-NVP, depending upon the side chain substitution. The MRR values are discussed in terms of monomer structural properties such as electronegativity and electron delocalization. The sequence distribution of monomers in the copolymers was studied by statistical method based on the average reactivity ratios obtained by EK-T method.
Journal
"Macromolecular Research" – Springer Journals
Published: Dec 1, 2009