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Co-Crystal of Phenylsuccinic Acid and 4,4'-Bipyridine: Synthesis, Characterization, Crystal Structure, and Supramolecular Interactions

Co-Crystal of Phenylsuccinic Acid and 4,4'-Bipyridine: Synthesis, Characterization, Crystal... A new co-crystal compound of 4,4'-bipyridine and phenylsuccinic acid was synthesized and characterized by elemental analysis, infrared and ultraviolet–visible spectroscopy, and X-ray single crystal diffraction. Crystallographic data for the compound was collected at 150(2) K. The synthesized compound is crystallized in the monoclinic system with the space group P21/n and unit cell parameters a = 9.3668(4), b = 18.5075(9), c = 11.1156(5) Å, β = 113.892(2)°. Complicated hydrogen bonding network (O–H···N, C–H···O) accompanied with the C–H···π stacking interaction leads to the formation of 3D supramolecular structure. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Crystallography Reports Springer Journals

Co-Crystal of Phenylsuccinic Acid and 4,4'-Bipyridine: Synthesis, Characterization, Crystal Structure, and Supramolecular Interactions

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References (23)

Publisher
Springer Journals
Copyright
Copyright © Pleiades Publishing, Inc. 2019
ISSN
1063-7745
eISSN
1562-689X
DOI
10.1134/S1063774519070125
Publisher site
See Article on Publisher Site

Abstract

A new co-crystal compound of 4,4'-bipyridine and phenylsuccinic acid was synthesized and characterized by elemental analysis, infrared and ultraviolet–visible spectroscopy, and X-ray single crystal diffraction. Crystallographic data for the compound was collected at 150(2) K. The synthesized compound is crystallized in the monoclinic system with the space group P21/n and unit cell parameters a = 9.3668(4), b = 18.5075(9), c = 11.1156(5) Å, β = 113.892(2)°. Complicated hydrogen bonding network (O–H···N, C–H···O) accompanied with the C–H···π stacking interaction leads to the formation of 3D supramolecular structure.

Journal

Crystallography ReportsSpringer Journals

Published: Dec 25, 2019

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