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- Publisher
- Springer Journals
- Copyright
- Copyright © The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2022
- ISSN
- 1040-7278
- eISSN
- 1572-8862
- DOI
- 10.1007/s10876-022-02263-0
- Publisher site
- See Article on Publisher Site
Abstract
Zinc(II) and cadmium(II) complexation with the dodecahydrido-closo-dodecaborate anion [B12H12]2– in the presence of benzimidazole ligands 1-methylbenzimidazo-2-yl-methyleneaniline (L1) and 1-ethyl-2-(4-methoxyphenyl)azobenzimidazole (L2) was studied. A number of Zn(II) and Cd(II) complexes with the [B12H12]2– anion and ligands L1 or L2 were obtained and characterized. Effect of the metal nature on the composition and structure of the resulting compounds was determined. Only tris-chelate zinc(II) complexes with the [B12H12]2– anion were isolated. For cadmium, first examples of mixed-ligand complexes with the [B12H12]2– anion coordinated by the metal atom via 3c2e (CdHB) bonds were isolated. Structures of complexes [Zn(L1)3][B12H12]·2CH3CN, [Cd(L1)2[B12H12]]·2CH3CN and [Cd(L2)2(CH3CN)[B12H12]]·CH3CN were determined by X-ray diffraction.Graphical Abstract[graphic not available: see fulltext]
Journal
Journal of Cluster Science – Springer Journals
Published: Mar 1, 2023
Keywords: Boron clusters; Mixed-ligand complexes; X-ray diffraction