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A facile and practical Amination of 4-Fluoronitrobenzene in continuous flow

A facile and practical Amination of 4-Fluoronitrobenzene in continuous flow A highly efficient protocol for the amination of 4-fluoronitrobenzene by using methylamine aqueous solution as the amination reagent was developed. The reaction proceeds smoothly to provide the desired product in high yield and excellent purity within 15 min at 70 °C. The particle size of the product obtained in this approach was less than 100 μm. And the reaction media exhibited excellent reusability after recovering four times.Graphical abstractA Facile and Practical Amination of 4-Fluoronitrobenzene in Continuous Flow. A highly efficient protocol for the amination of 4-fluoronitrobenzene by using methylamine aqueous solution as the amination reagent was developed. The particle size of the product obtained in this approach was less than 100 μm.[graphic not available: see fulltext] http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Journal of Flow Chemistry Springer Journals

A facile and practical Amination of 4-Fluoronitrobenzene in continuous flow

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Publisher
Springer Journals
Copyright
Copyright © Akadémiai Kiadó 2020
ISSN
2062-249X
eISSN
2063-0212
DOI
10.1007/s41981-019-00075-4
Publisher site
See Article on Publisher Site

Abstract

A highly efficient protocol for the amination of 4-fluoronitrobenzene by using methylamine aqueous solution as the amination reagent was developed. The reaction proceeds smoothly to provide the desired product in high yield and excellent purity within 15 min at 70 °C. The particle size of the product obtained in this approach was less than 100 μm. And the reaction media exhibited excellent reusability after recovering four times.Graphical abstractA Facile and Practical Amination of 4-Fluoronitrobenzene in Continuous Flow. A highly efficient protocol for the amination of 4-fluoronitrobenzene by using methylamine aqueous solution as the amination reagent was developed. The particle size of the product obtained in this approach was less than 100 μm.[graphic not available: see fulltext]

Journal

Journal of Flow ChemistrySpringer Journals

Published: Jun 25, 2020

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