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X-ray reflection curves of crystals with randomly distributed microdefects in the Bragg case

X-ray reflection curves of crystals with randomly distributed microdefects in the Bragg case The formalism of the optical coherence has been applied to the description of the Bragg-case dynamical X-ray diffraction from crystals with randomly distributed amorphous spheres. Explicit formulas have been found for the reflection curves of such crystals in the first and second approximations of the iterative solution of the Takagi equations. It is shown that if the coherent plane wave falls on the crystal the diffracted wave consists of two parts - the plane coherent wave (which corresponds to the diffraction from a perfect crystal with a modified value of the Debye-Waller factor) and the partially coherent wave (diffusion scattering). The form of the partially coherent contribution to the reflection curve is discussed and its dependence on the defect diameter and the defect concentration. From the curves the integrated intensities are obtained. It is proved that the integrated intensity of the waves diffracted from such crystals depends linearly on the relative disturbed volume of the crystal and in the first approximation it does not depend on the defect diameter if this volume remains constant. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Acta Crystallographica Section A: Foundations of Crystallography International Union of Crystallography

X-ray reflection curves of crystals with randomly distributed microdefects in the Bragg case

X-ray reflection curves of crystals with randomly distributed microdefects in the Bragg case


Abstract

The formalism of the optical coherence has been applied to the description of the Bragg-case dynamical X-ray diffraction from crystals with randomly distributed amorphous spheres. Explicit formulas have been found for the reflection curves of such crystals in the first and second approximations of the iterative solution of the Takagi equations. It is shown that if the coherent plane wave falls on the crystal the diffracted wave consists of two parts - the plane coherent wave (which corresponds to the diffraction from a perfect crystal with a modified value of the Debye-Waller factor) and the partially coherent wave (diffusion scattering). The form of the partially coherent contribution to the reflection curve is discussed and its dependence on the defect diameter and the defect concentration. From the curves the integrated intensities are obtained. It is proved that the integrated intensity of the waves diffracted from such crystals depends linearly on the relative disturbed volume of the crystal and in the first approximation it does not depend on the defect diameter if this volume remains constant.

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References (1)

Publisher
International Union of Crystallography
Copyright
Copyright (c) 1983 International Union of Crystallography
ISSN
0108-7673
DOI
10.1107/S0108767383001312
Publisher site
See Article on Publisher Site

Abstract

The formalism of the optical coherence has been applied to the description of the Bragg-case dynamical X-ray diffraction from crystals with randomly distributed amorphous spheres. Explicit formulas have been found for the reflection curves of such crystals in the first and second approximations of the iterative solution of the Takagi equations. It is shown that if the coherent plane wave falls on the crystal the diffracted wave consists of two parts - the plane coherent wave (which corresponds to the diffraction from a perfect crystal with a modified value of the Debye-Waller factor) and the partially coherent wave (diffusion scattering). The form of the partially coherent contribution to the reflection curve is discussed and its dependence on the defect diameter and the defect concentration. From the curves the integrated intensities are obtained. It is proved that the integrated intensity of the waves diffracted from such crystals depends linearly on the relative disturbed volume of the crystal and in the first approximation it does not depend on the defect diameter if this volume remains constant.

Journal

Acta Crystallographica Section A: Foundations of CrystallographyInternational Union of Crystallography

Published: Sep 1, 1983

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