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Treatment of secondary extinction and multiple scattering in polarized neutron scattering: an improved method. II. Application to nickel

Treatment of secondary extinction and multiple scattering in polarized neutron scattering: an... The flipping ratios for polarized neutron scattering from the first six reflections in Ni have been measured on a series of samples of varying thickness and perfection and at a number of wavelengths. The results were corrected for secondary extinction on a point-by-point basis, using the measured absolute reflectivities, and multiple scattering was detected using conservation of neutrons. No adjustable parameters were used, and all data, except those from a rather perfect specimen which showed both primary and secondary extinction, agree to within the experimental accuracy after extinction correction. A diffuse scattering process with spin dependence was also detected, and the flipping ratios corrected for this. The corrected values differ somewhat from the values given by Mook Phys. Rev. (1966), 14B, 495-501. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Acta Crystallographica Section A: Foundations of Crystallography International Union of Crystallography

Treatment of secondary extinction and multiple scattering in polarized neutron scattering: an improved method. II. Application to nickel

Treatment of secondary extinction and multiple scattering in polarized neutron scattering: an improved method. II. Application to nickel


Abstract

The flipping ratios for polarized neutron scattering from the first six reflections in Ni have been measured on a series of samples of varying thickness and perfection and at a number of wavelengths. The results were corrected for secondary extinction on a point-by-point basis, using the measured absolute reflectivities, and multiple scattering was detected using conservation of neutrons. No adjustable parameters were used, and all data, except those from a rather perfect specimen which showed both primary and secondary extinction, agree to within the experimental accuracy after extinction correction. A diffuse scattering process with spin dependence was also detected, and the flipping ratios corrected for this. The corrected values differ somewhat from the values given by Mook Phys. Rev. (1966), 14B, 495-501.

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References (1)

Publisher
International Union of Crystallography
Copyright
Copyright (c) 1984 International Union of Crystallography
ISSN
0108-7673
DOI
10.1107/S0108767384000052
Publisher site
See Article on Publisher Site

Abstract

The flipping ratios for polarized neutron scattering from the first six reflections in Ni have been measured on a series of samples of varying thickness and perfection and at a number of wavelengths. The results were corrected for secondary extinction on a point-by-point basis, using the measured absolute reflectivities, and multiple scattering was detected using conservation of neutrons. No adjustable parameters were used, and all data, except those from a rather perfect specimen which showed both primary and secondary extinction, agree to within the experimental accuracy after extinction correction. A diffuse scattering process with spin dependence was also detected, and the flipping ratios corrected for this. The corrected values differ somewhat from the values given by Mook Phys. Rev. (1966), 14B, 495-501.

Journal

Acta Crystallographica Section A: Foundations of CrystallographyInternational Union of Crystallography

Published: Jan 1, 1984

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