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Electron diffraction patterns of chrysotile: effect of specimen orientation

Electron diffraction patterns of chrysotile: effect of specimen orientation Electron diffraction patterns of chrysotile asbestos fibrils should have the 2mm symmetry of a rotation photograph because the layers in the structure are curled as cylinders. The way in which the fibril orientation affects the diffraction patterns is considered theoretically. The departures from ideal symmetry attributable to specimen orientation are noted: they affect mainly the h00 reflections close to the fibre axis. Actual diffraction patterns show a consistent difference in the separation of the h0l-h0 pairs on the upper levels, and 0l-0 pairs on the lower. The experimental conclusion Yada (1979). Can. Mineral. 17, 679-691 that this difference is not an effect of specimen orientation is confirmed theoretically but its cause remains obscure. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Acta Crystallographica Section A: Foundations of Crystallography International Union of Crystallography

Electron diffraction patterns of chrysotile: effect of specimen orientation

Electron diffraction patterns of chrysotile: effect of specimen orientation


Abstract

Electron diffraction patterns of chrysotile asbestos fibrils should have the 2mm symmetry of a rotation photograph because the layers in the structure are curled as cylinders. The way in which the fibril orientation affects the diffraction patterns is considered theoretically. The departures from ideal symmetry attributable to specimen orientation are noted: they affect mainly the h00 reflections close to the fibre axis. Actual diffraction patterns show a consistent difference in the separation of the h0l-h0 pairs on the upper levels, and 0l-0 pairs on the lower. The experimental conclusion Yada (1979). Can. Mineral. 17, 679-691 that this difference is not an effect of specimen orientation is confirmed theoretically but its cause remains obscure.

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References (4)

Publisher
International Union of Crystallography
Copyright
Copyright (c) 1988 International Union of Crystallography
ISSN
0108-7673
eISSN
1600-5724
DOI
10.1107/S0108767387009267
Publisher site
See Article on Publisher Site

Abstract

Electron diffraction patterns of chrysotile asbestos fibrils should have the 2mm symmetry of a rotation photograph because the layers in the structure are curled as cylinders. The way in which the fibril orientation affects the diffraction patterns is considered theoretically. The departures from ideal symmetry attributable to specimen orientation are noted: they affect mainly the h00 reflections close to the fibre axis. Actual diffraction patterns show a consistent difference in the separation of the h0l-h0 pairs on the upper levels, and 0l-0 pairs on the lower. The experimental conclusion Yada (1979). Can. Mineral. 17, 679-691 that this difference is not an effect of specimen orientation is confirmed theoretically but its cause remains obscure.

Journal

Acta Crystallographica Section A: Foundations of CrystallographyInternational Union of Crystallography

Published: Jan 1, 1988

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