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Density-functional theory of atoms and molecules
- Publisher
- de Gruyter
- Copyright
- ©2016 by De Gruyter
- ISSN
- 0932-0776
- eISSN
- 1865-7117
- DOI
- 10.1515/znb-2015-0076
- Publisher site
- See Article on Publisher Site
Abstract
AbstractA variety of N-acyl-N-(4-chlorophenyl)-4-nitrobenzenesulfonamides (1a–e) were synthesized in one pot from 4-chloroaniline under solvent-free conditions and have been developed as chemoselective N-acylation reagents. Selective protection of primary amines in the presence of secondary amines, acylation of aliphatic amines in the presence of aryl amines, and monofunctionalization of primary-secondary diamines as well as selective N-acylation of amino alcohols using these reagents are described. All of the acylation reactions were carried out in water as a green solvent. High stability and easy preparation of these acylating reagents are other advantages of this method.
Journal
Zeitschrift für Naturforschung B – de Gruyter
Published: Feb 1, 2016