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Y. Qi, S. Harris (2010)
In Situ Observation of Strains during Lithiation of a Graphite ElectrodeJournal of The Electrochemical Society, 157
V. Yufit, P. Shearing, R. Hamilton, P. Lee, M. Wu, N. Brandon (2011)
Investigation of lithium-ion polymer battery cell failure using X-ray computed tomographyElectrochemistry Communications, 13
F. Zernike (1942)
Phase contrast, a new method for the microscopic observation of transparent objectsPhysica D: Nonlinear Phenomena, 9
J. Hubbell, S. Seltzer (1995)
Tables of X-Ray Mass Attenuation Coefficients and Mass Energy-Absorption Coefficients 1 keV to 20 MeV for Elements Z = 1 to 92 and 48 Additional Substances of Dosimetric Interest
Syue-Ren Wu, Y. Hwu, G. Margaritondo (2012)
Hard-X-ray Zone Plates: Recent ProgressMaterials, 5
P. Pietsch, M. Hess, W. Ludwig, J. Eller, V. Wood (2016)
Combining operando synchrotron X-ray tomographic microscopy and scanning X-ray diffraction to study lithium ion batteriesScientific Reports, 6
M. Ebner, F. Marone, M. Stampanoni, V. Wood (2013)
Visualization and Quantification of Electrochemical and Mechanical Degradation in Li Ion BatteriesScience, 342
T. Weitkamp, D. Haas, D. Haas, D. Wȩgrzynek, A. Rack (2011)
ANKAphase: software for single-distance phase retrieval from inline X-ray phase-contrast radiographs.Journal of synchrotron radiation, 18 Pt 4
Naoki Nitta, Feixiang Wu, Jung Lee, G. Yushin (2015)
Li-ion battery materials: present and futureMaterials Today, 18
C. Aggarwal, C. Reddy (2013)
Data Clustering
James Wilson, J. Cronin, S. Barnett, S. Harris (2011)
Measurement of three-dimensional microstructure in a LiCoO2 positive electrodeJournal of Power Sources, 196
M. Ender, Jochen Joos, T. Carraro, E. Ivers-Tiffée (2011)
Three-dimensional reconstruction of a composite cathode for lithium-ion cellsElectrochemistry Communications, 13
Ali Kashkooli, Siamak Farhad, D. Lee, Kun Feng, S. Litster, S. Babu, Likun Zhu, Zhongwei Chen (2016)
Multiscale modeling of lithium-ion battery electrodes based on nano-scale X-ray computed tomographyJournal of Power Sources, 307
Feifei Yang, Yijin Liu, S. Martha, Ziyu Wu, J. Andrews, G. Ice, P. Pianetta, J. Nanda (2014)
Nanoscale Morphological and Chemical Changes of High Voltage Lithium–Manganese Rich NMC Composite Cathodes with CyclingNano Letters, 14
P. Reischig, A. King, Laura Nervo, N. Viganò, Y. Guilhem, W. Palenstijn, K. Batenburg, M. Preuss, W. Ludwig (2013)
Advances in X-ray diffraction contrast tomography: Flexibility in the setup geometry and application to multiphase materialsJournal of Applied Crystallography, 46
J. Nelson, Yuan Yang, S. Misra, J. Andrews, Yi Cui, M. Toney (2013)
Identifying and managing radiation damage during in situ transmission x-ray microscopy of Li-ion batteries, 8851
J. Als-Nielsen, D. McMorrow (2011)
Elements of Modern X-ray Physics: Als-Nielsen/Elements
J. Hubbell, H. Gimm, I. Oeverboe (1980)
Pair, Triplet, and Total Atomic Cross Sections (and Mass Attenuation Coefficients) for 1 MeV-100 GeV Photons in Elements Z=1 to 100,Journal of Physical and Chemical Reference Data, 9
A. Latz, J. Zausch (2015)
Multiscale modeling of lithium ion batteries: thermal aspectsBeilstein Journal of Nanotechnology, 6
M. Bech (2010)
X-Ray Imaging with a Grating Interferometer
L. Zielke, C. Barchasz, S. Walus, F. Alloin, J. Leprêtre, A. Spettl, V. Schmidt, A. Hilger, I. Manke, J. Banhart, R. Zengerle, S. Thiele (2015)
Degradation of Li/S Battery Electrodes On 3D Current Collectors Studied Using X-ray Phase Contrast TomographyScientific Reports, 5
L. Grodzins (1983)
Optimum energies for x-ray transmission tomography of small samples. Applications of synchrotron radiation to computerized tomography INuclear Instruments and Methods in Physics Research, 206
J. Weker, Nian Liu, S. Misra, J. Andrews, Yi Cui, Yi Cui, M. Toney (2014)
In situ nanotomography and operando transmission X-ray microscopy of micron-sized Ge particlesEnergy and Environmental Science, 7
Fu Sun, L. Zielke, H. Markötter, A. Hilger, D. Zhou, R. Moroni, R. Zengerle, S. Thiele, J. Banhart, I. Manke (2016)
Morphological Evolution of Electrochemically Plated/Stripped Lithium Microstructures Investigated by Synchrotron X-ray Phase Contrast Tomography.ACS nano, 10 8
M. Ender, Jochen Joos, A. Weber, E. Ivers-Tiffée (2014)
Anode microstructures from high-energy and high-power lithium-ion cylindrical cells obtained by X-ray nano-tomographyJournal of Power Sources, 269
C. Villevieille, M. Ebner, J. Gómez‐Cámer, F. Marone, P. Novák, V. Wood (2015)
Influence of Conversion Material Morphology on Electrochemistry Studied with Operando X‐Ray Tomography and DiffractionAdvanced Materials, 27
B. Vijayaraghavan, D. Ely, Y. Chiang, R. García-García, R. García (2012)
An Analytical Method to Determine Tortuosity in Rechargeable Battery ElectrodesJournal of The Electrochemical Society, 159
Tim Mitsch, Yvonne Krämer, J. Feinauer, G. Gaiselmann, H. Markötter, I. Manke, A. Hintennach, V. Schmidt (2014)
Preparation and Characterization of Li-Ion Graphite Anodes Using Synchrotron TomographyMaterials, 7
G. Herman (2009)
Fundamentals of Computerized Tomography: Image Reconstruction from Projections
B. Henke, E. Gullikson, J. Davis (1993)
X-Ray Interactions: Photoabsorption, Scattering, Transmission, and Reflection at E = 50-30,000 eV, Z = 1-92Atomic Data and Nuclear Data Tables, 54
S. Cooper, D. Eastwood, J. Gelb, Gaetan Damblanc, D. Brett, R. Bradley, P. Withers, P. Lee, A. Marquis, N. Brandon, P. Shearing (2014)
Image based modelling of microstructural heterogeneity in LiFePO4 electrodes for Li-ion batteriesJournal of Power Sources, 247
S. Harris, Peng Lu (2013)
Effects of Inhomogeneities—Nanoscale to Mesoscale—on the Durability of Li-Ion BatteriesJournal of Physical Chemistry C, 117
Y. Chen‐Wiegart, P. Shearing, Qing-xin Yuan, A. Tkachuk, Jun Wang (2012)
3D morphological evolution of Li-ion battery negative electrode LiVO2 during oxidation using X-ray nano-tomographyElectrochemistry Communications, 21
M. Ebner, V. Wood (2015)
Tool for Tortuosity Estimation in Lithium Ion Battery Porous ElectrodesJournal of The Electrochemical Society, 162
J. Gonzalez, K. Sun, Meng Huang, J. Lambros, S. Dillon, I. Chasiotis (2014)
Three dimensional studies of particle failure in silicon based composite electrodes for lithium ion batteriesJournal of Power Sources, 269
M. Ebner, Felix Geldmacher, F. Marone, M. Stampanoni, V. Wood (2013)
X‐Ray Tomography of Porous, Transition Metal Oxide Based Lithium Ion Battery ElectrodesAdvanced Energy Materials, 3
J. Paz-García, Oluwadamilola Taiwo, Erika Tudisco, D. Finegan, P. Shearing, D. Brett, S. Hall (2016)
4D analysis of the microstructural evolution of Si-based electrodes during lithiation: Time-lapse X-ray imaging and digital volume correlationJournal of Power Sources, 320
M. Ebner, D. Chung, R. García, V. Wood (2014)
Tortuosity Anisotropy in Lithium‐Ion Battery ElectrodesAdvanced Energy Materials, 4
F. Meirer, J. Cabana, Yijin Liu, A. Mehta, J. Andrews, P. Pianetta (2011)
Three-dimensional imaging of chemical phase transformations at the nanoscale with full-field transmission X-ray microscopy.Journal of synchrotron radiation, 18 Pt 5
D. Paganin, S. Mayo, T. Gureyev, P. Miller, S. Wilkins (2002)
Simultaneous phase and amplitude extraction from a single defocused image of a homogeneous objectJournal of Microscopy, 206
D. Finegan, Erika Tudisco, M. Scheel, J. Robinson, Oluwadamilola Taiwo, D. Eastwood, P. Lee, M. Michiel, B. Bay, S. Hall, G. Hinds, D. Brett, P. Shearing (2015)
Quantifying Bulk Electrode Strain and Material Displacement within Lithium Batteries via High‐Speed Operando Tomography and Digital Volume CorrelationAdvanced Science, 3
D. Kehrwald, P. Shearing, N. Brandon, P. Sinha, S. Harris (2011)
Local Tortuosity Inhomogeneities in a Lithium Battery Composite ElectrodeJournal of The Electrochemical Society, 158
Guangmin Zhou, S. Pei, Lu Li, Da‐Wei Wang, Shaogang Wang, Kun-Ping Huang, L. Yin, Feng Li, Hui‐Ming Cheng (2014)
A Graphene–Pure‐Sulfur Sandwich Structure for Ultrafast, Long‐Life Lithium–Sulfur BatteriesAdvanced Materials, 26
Mehmet Sezgin, B. Sankur (2004)
Survey over image thresholding techniques and quantitative performance evaluationJ. Electronic Imaging, 13
L. Zielke, Fu Sun, H. Markötter, A. Hilger, R. Moroni, R. Zengerle, S. Thiele, J. Banhart, I. Manke (2016)
Synchrotron X‐ray tomographic study of a silicon electrode before and after discharge and the effect of cavities on particle fracturing, 3
S. Babu, A. Mohamed, J. Whitacre, S. Litster (2015)
Multiple imaging mode X-ray computed tomography for distinguishing active and inactive phases in lithium-ion battery cathodesJournal of Power Sources, 283
I. Manke, J. Banhart, A. Haibel, A. Rack, S. Zabler, N. Kardjilov, A. Hilger, A. Melzer, H. Riesemeier (2007)
In situ investigation of the discharge of alkaline Zn–MnO2 batteries with synchrotron x-ray and neutron tomographiesApplied Physics Letters, 90
D. Eastwood, P. Bayley, H. Chang, Oluwadamilola Taiwo, J. Vila-Comamala, D. Brett, C. Rau, P. Withers, P. Shearing, C. Grey, P. Lee (2015)
Three-dimensional characterization of electrodeposited lithium microstructures using synchrotron X-ray phase contrast imaging.Chemical communications, 51 2
Y. Chen‐Wiegart, Ross Demike, C. Erdonmez, K. Thornton, S. Barnett, Jun Wang (2014)
Tortuosity characterization of 3D microstructure at nano-scale for energy storage and conversion materialsJournal of Power Sources, 249
Wim Aarle, W. Palenstijn, J. Beenhouwer, T. Altantzis, S. Bals, K. Batenburg, Jan Sijbers (2015)
The ASTRA Toolbox: A platform for advanced algorithm development in electron tomography.Ultramicroscopy, 157
S. McDonald, F. Marone, C. Hintermüller, G. Mikuljan, C. David, F. Pfeiffer, M. Stampanoni (2009)
Advanced phase-contrast imaging using a grating interferometer.Journal of synchrotron radiation, 16 Pt 4
A. King, A. King, G. Johnson, G. Johnson, D. Engelberg, W. Ludwig, J. Marrow (2008)
Observations of Intergranular Stress Corrosion Cracking in a Grain-Mapped PolycrystalScience, 321
P. Shearing, L. Howard, P. Jørgensen, N. Brandon, S. Harris (2010)
Characterization of the 3-dimensional microstructure of a graphite negative electrode from a Li-ion batteryElectrochemistry Communications, 12
A. Kak, M. Slaney (2001)
Principles of computerized tomographic imaging, 33
S. Stock (2008)
Recent advances in X-ray microtomography applied to materialsInternational Materials Reviews, 53
R. Mokso, F. Marone, S. Irvine, M. Nývlt, D. Schwyn, K. Mader, G. Taylor, H. Krapp, M. Škereň, M. Stampanoni (2013)
Advantages of phase retrieval for fast x-ray tomographic microscopyJournal of Physics D: Applied Physics, 46
Farid Tariq, V. Yufit, D. Eastwood, Yu Merla, M. Biton, Billy Wu, Zhangwei Chen, K. Freedman, G. Offer, E. Peled, P. Lee, D. Golodnitsky, N. Brandon (2014)
In-Operando X-ray Tomography Study of Lithiation Induced Delamination of Si Based Anodes for Lithium-Ion BatteriesECS Electrochemistry Letters, 3
D. Finegan, M. Scheel, J. Robinson, Bernhard Tjaden, I. Hunt, T. Mason, J. Millichamp, M. Michiel, G. Offer, G. Hinds, D. Brett, P. Shearing (2015)
In-operando high-speed tomography of lithium-ion batteries during thermal runawayNature Communications, 6
P. Pietsch, D. Westhoff, J. Feinauer, J. Eller, F. Marone, M. Stampanoni, V. Schmidt, V. Wood (2016)
Quantifying microstructural dynamics and electrochemical activity of graphite and silicon-graphite lithium ion battery anodesNature Communications, 7
Simon Hein, A. Latz (2016)
Influence of local lithium metal deposition in 3D microstructures on local and global behavior of Lithium-ion batteriesElectrochimica Acta, 201
Farid Tariq, V. Yufit, M. Kishimoto, P. Shearing, S. Menkin, D. Golodnitsky, J. Gelb, E. Peled, N. Brandon (2014)
Three-dimensional high resolution X-ray imaging and quantification of lithium ion battery mesocarbon microbead anodesJournal of Power Sources, 248
E. Maire, P. Withers (2014)
Quantitative X-ray tomographyInternational Materials Reviews, 59
Feng Lin, Isaac Markus, M. Doeff, H. Xin (2014)
Chemical and Structural Stability of Lithium-Ion Battery Electrode Materials under Electron BeamScientific Reports, 4
M. Lagadec, M. Ebner, R. Zahn, V. Wood (2016)
Communication—Technique for Visualization and Quantification of Lithium-Ion Battery Separator MicrostructureJournal of The Electrochemical Society, 163
Johanna Weker, M. Toney (2015)
Emerging In Situ and Operando Nanoscale X‐Ray Imaging Techniques for Energy Storage MaterialsAdvanced Functional Materials, 25
L. Steinbock, C. Dustmann (2001)
Investigation of the Inner Structures of ZEBRA Cells with a MicrotomographJournal of The Electrochemical Society, 148
D. Eastwood, R. Bradley, Farid Tariq, S. Cooper, Oluwadamilola Taiwo, J. Gelb, A. Merkle, D. Brett, N. Brandon, P. Withers, P. Lee, P. Shearing (2014)
The application of phase contrast X-ray techniques for imaging Li-ion battery electrodesNuclear Instruments & Methods in Physics Research Section B-beam Interactions With Materials and Atoms, 324
D. Eastwood, V. Yufit, J. Gelb, A. Gu, R. Bradley, S. Harris, D. Brett, N. Brandon, Peter Lee, P. Withers, P. Shearing (2014)
Lithiation‐Induced Dilation Mapping in a Lithium‐Ion Battery Electrode by 3D X‐Ray Microscopy and Digital Volume CorrelationAdvanced Energy Materials, 4
P. Shearing, N. Brandon, J. Gelb, R. Bradley, P. Withers, A. Marquis, S. Cooper, S. Harris (2012)
Multi Length Scale Microstructural Investigations of a Commercially Available Li-Ion Battery ElectrodeJournal of The Electrochemical Society, 159
L. Zielke, T. Hutzenlaub, D. Wheeler, I. Manke, T. Arlt, N. Paust, R. Zengerle, S. Thiele (2014)
A Combination of X‐Ray Tomography and Carbon Binder Modeling: Reconstructing the Three Phases of LiCoO2 Li‐Ion Battery CathodesAdvanced Energy Materials, 4
J. Gonzalez, K. Sun, Meng Huang, S. Dillon, I. Chasiotis, J. Lambros (2015)
X-ray microtomography characterization of Sn particle evolution during lithiation/delithiation in lithium ion batteriesJournal of Power Sources, 285
J. Als-Nielsen, D. McMorrow (2001)
Elements of Modern X-ray Physics
M. Langer, P. Cloetens, J. Guigay, F. Peyrin (2008)
Quantitative comparison of direct phase retrieval algorithms in in-line phase tomography.Medical physics, 35 10
X-ray tomography has emerged as a powerful technique for studying lithium ion batteries, allowing nondestructive and often quantitative imaging of these complex systems, which contain solid components with length scales spanning orders of magnitude and which are in-filled with liquid electrolyte. Over the past decade, X-ray tomography has allowed interrogation of structure and material composition, providing quantitative or qualitative insight into battery operation and degradation. In this review, we first provide an overview of X-ray tomography and explore what types of experiments can yield insight into open questions in the lithium ion battery research field. In the second half of the review, we discuss the aspects a researcher must consider, and we summarize challenges and approaches to sample preparation, experimental setup, and data analysis. Finally, we describe both outstanding challenges and promise in using X-ray tomography for lithium ion battery research.
Annual Review of Materials Research – Annual Reviews
Published: Jul 3, 2017
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