11 - 16 of 16 articles
This article investigates the formation process of double emulsions, controlling their sizes, and manipulating the encapsulation process in a three nested microcapillary tube configuration. In the proposed geometry, as a result of the interaction of liquids using dripping instability, double...
In this work, the method of combining the various ligands with Raney Ni in continuous flow is proposed, in which triphenylphosphine (TPP) can effectively improve the chemical selectivity of anilines prepared by nitroarenes hydrogenation and maintain high activity. Meanwhile, through the analysis...
This study presents a robust and scalable method for synthesizing continuously the silica microspheres via the Stöber method. Owing to the superb mixing accessible with gas-liquid segmented flow in coiled microtube, satisfactory morphology and mono-dispersity of silica spheres was obtained. The...
The process characteristics of two main steps in the preparation of 4-nitrobiphenyl (4-NBP) from 4-nitroaniline (PNA) were clearly revealed by applying two continuous-flow microreactors. The first step was the synthesis of 4-nitrobenzene diazonium tetrafluoroborate (4-NBDT) through the...
Here we developed a continuous flow microreactor system to synthesis N-benzoylpiperazine, which is an important intermediate of novel nootropic Sunifiram. And the kinetics of the condensation amidation of piperazine and benzoic acid using HATU as coupling reagent was revealed in microreactor. A...
Reversible addition-fragmentation chain transfer radical polymerization of styrene and maleic anhydride was successfully performed in continuous-flow microreactor. Results of the structural characterization showed that the obtained styrene-maleic anhydride (SMA) copolymers possessed controlled...
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