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Reaction of 1-phthalazinylhydrazone of o-diphenylphosphinobenzaldehyde (HL) with Fe(II) and Co(II) perchlorates has led to complexes of different composition and structure: [Fe(HL)2](ClO4)2 · H2O (1) and [CoL2](ClO4) · H2O (2) in spite of the use of salts with the same anion. Со2+ ion undergoes...
A method has been developed for synthesizing composites of titanium oxide nanoparticles (anatase and rutile) on the surface of reduced graphene oxide flakes in supercritical isopropanol. Supercritical isopropanol acts in synthesis not only as a reducing agent but also as a reaction medium, while...
Ultra-high-temperature Ta4HfC5 ceramics with a submicron structure has been manufactured from a 4Ta + Hf + 5С powder mixture by electro-thermal explosion under pressure. The effect of the duration of mechanical activation of starting 4Ta + Hf powder mixtures on the structure of the resulting...
Carbon nanofibers obtained by catalytic decomposition of methane in a vibrated fluidized bed reactor were chemically treated to increase the specific capacitance of supercapacitors. The material was studied by transmission electron microscopy, energy dispersive X-ray spectroscopy, Fourier...
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