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A photoredox catalytic synthesis of functionalized 2‐aminofurans is proposed starting from α‐halo carbonyl substrates and N‐allenamides. The protocol proves to be efficient and sustainable thanks to: i) the use of visible light as green energy source, ii) the redox‐neutral nature of the...
Electrochemical synthesis offers a mild, simple, and efficient tool for the preparation of interesting and useful molecules, thus eluding severe chemical oxidizing and reducing agents used in conventional synthetic methods. In particular, electrochemical C−H activation is expected to play an...
γ‐Amino esters and γ‐lactams containing α,γ‐stereogenic centers are widely used as chiral intermediates in various bioactive compounds, while their efficient synthesis remains a challenge. Herein, an enzymatic cascade reaction involving an ene reductase (ERED) and an imine reductase (IRED) for...
Palladium‐catalyzed (3+3) and (3+4) cycloannulations between vinylcyclopropanes and various (hetero)aromatic aldehydes are reported. The use of phosphonate‐substituted vinylcyclopropanes provides access to a variety of bi‐ or tricyclic heteroaromatic scaffolds via an allylation/olefination...
An iodine‐catalyzed double [4+2] oxidative annulation of ketones and diamines is described. A multi‐pathway coupled domino strategy has been developed for the synthesis of substituted dimeric pyrazines under metal‐free conditions. One C−C and four C−N bonds are formed during this double [4+2]...
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