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A low-cost facile synthesis of electronic nanomaterials such as magnetite (Fe3O4), and gold (Au) using polyvinylpyrrolidone (PVP) as a reducing and stabilizing agent in a 3D-printed droplet-based microfluidic device has been demonstrated. The nanomaterial synthesis in terms of obtaining...
In this study, m-xylene nitration was scaled up in a microreactor. The effects of temperature, molar ratio, and mass fraction of sulfuric acid on the two synthesis methods were systematically analyzed. The reaction temperature and mass fraction of sulfuric acid are the main factors influencing...
An expeditious and efficient continuous-flow process is reported for the synthesis of N,N′-bis(2,2,6,6-tetramethyl-4-piperidinyl)-1,6-hexanediamine (DTMPA). The starting material 1,6-hexanediamine (HMDA) mixes with 2,2,6,6-tetramethyl-4-piperidinone (TAA), reacts with hydrogen in a micro...
Palladium-catalyzed decarboxylative cross-coupling was employed to synthesize 2-arylpyrroles via a flow process. This reaction features palladium as the only metal catalyst and uses easily accessible starting materials. The reaction temperature, the residence time, and the quantity of different...
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