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Abstract A solvothermal continuous-flow method for the scalable and shape tunable synthesis of rod-like/spherical TiO2 nanocrystals (NCs) has been developed. The as-prepared colloidal NCs show photocatalytic activity in an addition-cyclization cascade under continuous-flow conditions.
Abstract An ultrasound irradiated continuous-flow system was developed to accelerate chemical reaction by cavitation effect. Nucleophilic aromatic substitutions were performed, and the results showed that ultrasound irradiated is superior over generic heating in a continuous-flow system. The...
Abstract Using mild conditions and short reaction times, symmetrical disulfides have been synthesized in flow chemistry using phase transfer catalysts to facilitate the substitution of organohalides with disodium disulfide. Also, the synthesis of symmetrical trisulfides was possible using this...
Abstract In this work, a three-step chemo enzymatic cascade reaction is reported for 1-monoacylglycerols from glycerol derived from biodiesel industry under continuous-flow conditions. Glycerol protection was performed using H2SO4/SiO2 (2.5 %w/v) solid catalyst and acetone, generating 87 % of...
Abstract The inner walls of a glass microreactor were functionalized in a one-step procedure with a single layer of a strong perfluoroalkylsulfonic acid. The applicability of the catalytic device was demonstrated in the successful hydrolysis of benzaldehyde dimethyl acetal in acetonitrile,...
Abstract In this section of the journal, the continuous-flow chemistry literature of the preceding months is presented. Included are articles published in the period July–September 2013. Some key examples are highlighted in the form of graphical abstracts. The remaining publications in the field...
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