1 - 6 of 6 articles
Abstract Au-Pt and Au-Pd bimetallic nanoclusters that catalyzed the aerobic oxidation of alcohols during a once-through pass through gas-liquid-liquid-solid flow systems were developed. Alcohols were converted to aldehydes and ketones in benzotrifluoride (BTF)/water media by Au-Pt catalyst or to...
Abstract O-Alkylation of phenol compounds was performed in a continuous flow apparatus under biphasic liquid/liquid conditions and promoted by tetrabutylammonium bromide (TBAB) as a phase-transfer catalyst. The segmented flow that is generated within the flow system is able to afford the desired...
Abstract Hydrazoic acid (HN3) was used in a safe and reliable way for the synthesis of 5-substitued-1H-tetrazoles and for the preparation of N-(2-azidoethyl)acylamides in a continuous flow format. Hydrazoic acid was generated in situ either from an aqueous feed of sodium azide upon mixing with...
Abstract The synthesis and utilisation of acyl azides in a flow apparatus combined with an automated extraction unit is described. This process safely provides multi-100 g quantities of a labile diacyl azide (3) as an intermediate that could not be generated safely by classic batch methods. Its...
Abstract This paper describes the next stage in our development of self-optimising reactors. We demonstrate that the same reaction can be optimised for a series of different criteria including yield, space-time yield, E factor and a weighted yield function (the product of space-time yield and...
Abstract In this section of the journal, the continuous flow chemistry literature of the preceding months is presented. The first part for the year 2012 includes articles published in the last 3 months of 2011. Some key examples are highlighted in the form of graphical abstracts. The remaining...
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